Investigation on the anti-reduction mechanism of Ti4+ in high dielectric constant system Ca0.9La0.067TiO3 by doping with Al2O3

Ca_0.9La_0.067TiO₃ (abbreviated as CLT) ceramics doped with different amount of Al₂O₃ were prepared via the solid state reaction method. The anti-reduction mechanism of Ti⁴⁺ in CLT ceramics was carefully investigated. X-ray diffraction (XRD) was used to analyze the phase composition and lattice structure. Meanwhile, the Rietveld method was taken to calculate the lattice parameters. X-ray photoelectron spectroscopy (XPS) was employed to study the valence variation of Ti ions in CLT ceramics without and with Al₂O₃. The results showed that Al³⁺ substituted for Ti⁴⁺ to form solid solution and the solid solubility limit of Al³⁺ is near 1.11 mol%. Furthermore, the reduction of Ti⁴⁺ in CLT ceramics was restrained by acceptor doping process and the Q × f values of CLT ceramics were improved significantly. The CLT ceramic doped with 1.11 mol% Al₂O₃ exhibited good microwave dielectric properties: ε_r = 141, Q × f = 6848 GHz, τ_f = 576 ppm/°C.     

沁水盆地赵庄矿3号煤层地面煤层气抽采低产原因分析

在对沁水盆地赵庄矿煤层气开发地质、煤层气生产井资料深入研究的基础上，分析、总结了区内煤层气直井低产原因，并据此提出了区内地面抽采后续开发方向。研究认为:3号煤层气含量偏低、含气饱和度低、临储比低，致使排采阶段气含量可降幅度低，是其低产的宏观表征；3号煤储层不匹配孔级，较差连通性，即微、小孔为主，中孔次之，大孔不发育，微裂隙连通性差，致使扩散缓慢、影响储层改造和抽采效果，是其低产的微观表征；3号煤层远高于顶底板塑性及相近的水平应力，进一步造成改造缝长受限，泄流面积不足。因此，建议区内后续地面抽采方式应以增大泄流面积开发方式为主。     

65号航空冷却液的泡沫倾向性研究

针对65号航空冷却液在过滤循环中出现泡沫较多的现象，对65号航空冷却液泡沫倾向性进行探究。按照石化行业标准《发动机冷却液泡沫倾向测定法（SH /T 0066-2002）》，利用冷却液泡沫倾向测定仪来评价65号航空冷却液泡沫倾向性，并进行水乙二醇溶液对照试验。结果表明，航空冷却液在低温和循环时间较长的情况下，其泡沫倾向性较大，而随着温度的升高和循环时间的缩短，泡沫倾向性有一定程度的改善；并且通过水乙二醇对照试验可知，冷却液的基础液泡沫倾向性较小。航空冷却液在过滤循环中出现的泡沫问题，是加入的添加剂所引起的。     

Discovery of New Antiproliferative Imidazopyrazole Acylhydrazones Able To Interact with Microtubule Systems

Even though immunotherapy has radically changed the search for anticancer therapies, there are still many different pathways that are open to intervention with traditional small molecules. To expand our investigation in the anticancer field, we report here a new series of compounds in which our previous pyrazole and imidazopyrazole scaffolds are linked to a differently decorated phenyl ring through an acylhydrazone linker. Preliminary tests on the library were performed at the National Cancer Institute (USA) against the full NCI 60 cell panel. The best compounds among the imidazopyrazole series were then tested by immunofluorescence staining for their inhibition of cell proliferation, apoptosis induction, and their effect on the cell cycle and on microtubules. Two compounds, in particular 4-benzyloxy-3-methoxybenzyliden imidazopyrazole-7-carbohydrazide showed good growth inhibition, with IC₅₀ values in the low-micromolar range, and induced apoptosis. Both compounds altered the cell-cycle phases with the appearance of polyploid cells. Immunofluorescence analysis evidenced microtubules alterations; tubulin polymerization assays and docking studies suggested the tubulin system to be the possible, although not exclusive, target of the new acylhydrazone series reported here.     

飞机机械成品试验信息管理系统设计与应用

分析了航空企业飞机机械成品试验的现状,结合企业信息化管理的发展趋势,对飞机机械成品试验的流程进行梳理,基于ASP.NET技术研究开发了某企业飞机机械成品试验数据收集及信息管理系统,以实现飞机机械成品试验的流程化、数字化及显性化管理,避免因试验台管理不善造成的质量问题,实时掌握试验台状态,促进形成自主管理模式。     

基于深度网络迁移学习的致痫区脑电识别* .txt

摘要：致痫区脑电识别能够为癫痫外科手术提供重要的参考价值。提出了一种基于深度网络迁移学习的致痫区脑电识别算法。首先利用连续小波变换（CWT）对脑电信号进行时频分析，获得脑电信号时频图；然后迁移学习AlexNet网络模型，调整网络结构使之适应于致痫区脑电识别，将模型第7层全连接层输出作为脑电信号时频图的特征表示，最后利用支持向量机（SVM）、BP神经网络、长短期记忆网络（LSTM）、基于稀疏表达分类算法（SRC）、线性判别分析（LDA）等分类算法进行特征分类。基于开源脑电数据集采用十折交叉验证的方法对算法进行了验证,比较6种分类器的效果，得到SVM算法的平均特异性为8881%，灵敏度为8807%，准确率为8844%，证明了该方法识别致痫区脑电信号的有效性。 .txt     

一种下肢运动意图识别算法性能实时测评系统* .txt

摘要：对腿部运动意图识别算法的实时性能进行综合可靠的评价是实现下肢假肢灵活稳定控制的前提。提出一种逐层分级的基于下肢运动意图识别算法的实时测评方法，对算法的可靠性、稳定性以及运动意图识别速度进行综合评价。利用开发的运动意图识别算法评测系统，对基于肌电信号源和机械信号源的两种运动意图识别算法进行了实时性能测试，发现肌电信号源的算法识别时间大于机械信号源算法，但是其算法稳定性优于机械信号源算法。进一步地，还利用该评测系统有效地区分出正常识别策略与异常识别策略，发现正常策略的动作识别稳定系数比异常策略高25%左右。因此，所提的基于下肢运动意图识别算法的实时测评方法，能够对不同信号源算法以及不同识别策略的实时性能进行有效评价，为智能下肢假肢控制系统开发提供可供参考的测试平台。 .txt     

Improving EBSD precision by orientation refinement with full pattern matching

We present a comparison of the precision of different approaches for orientation imaging using electron backscatter diffraction (EBSD) in the scanning electron microscope. We have used EBSD to image the internal structure of WC grains, which contain features due to dislocations and subgrains. We compare the conventional, Hough-transform based orientation results from the EBSD system software with results of a high-precision orientation refinement using simulated pattern matching at the full available detector resolution of 640 × 480 pixels. Electron channelling contrast imaging (ECCI) is used to verify the correspondence of qualitative ECCI features with the quantitative orientation data from pattern matching. For the investigated sample, this leads to an estimated pattern matching sensitivity of about 0.5 mrad (0.03°) and a spatial feature resolution of about 100 nm. In order to investigate the alternative approach of postprocessing noisy orientation data, we analyse the effects of two different types of orientation filters. Using reference features in the high-precision pattern matching results for comparison, we find that denoising of orientation data can reduce the spatial resolution, and can lead to the creation of orientation artefacts for crystallographic features near the spatial and orientational resolution limits of EBSD.     

Grain mapping to freeform surface for machining using parameter-based incremental tracking method

This paper presents a novel method for mapping a texture for machining onto a freeform surface. When a grain texture designed on a 2D plane is projected onto a freeform surface simply, the texture is distorted along the curvature of the surface in the projection direction. Therefore, a method is required to suppress this distortion. The algorithm proposed in this paper rapidly generates a point cloud that represents a texture with less distortion on a simply connected parametric surface. Specifically, four equations that express local geometry constraints instead of conventional parameterization methods are presented to reduce the distortion between adjacent points on the point cloud. Solving these equations can generate grain textures on freeform surfaces. This paper examines two grain images mapped to two freeform surfaces that were prepared as case studies to demonstrate the effectiveness of the proposed method.